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簡(jian)要描(miao)述(shu):分子蒸餾儀可(ke)代替常(chang)規(gui)降(jiang)膜蒸發(fa)器(qi),用(yong)於石(shi)化(hua)及(ji)化(hua)工產品(pin)的蒸餾、提純(chun)、濃(nong)縮(suo)、脫(tuo)色(se)使(shi)用(yong);尤其(qi)適(shi)用(yong)於熱(re)敏(min)性(xing),易(yi)氧化化(hua)學(xue)工(gong)業品(pin)的蒸餾精(jing)制(zhi);也(ye)可(ke)用(yong)於高(gao)沸點產品(pin)的蒸餾分離。
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分子蒸餾儀介(jie)紹Introduction To Molecular Distillation Unit:
分子蒸餾是壹(yi)種(zhong)特殊(shu)的液(ye)—液(ye)分(fen)離技術,它不同於傳統蒸餾依靠(kao)沸點差(cha)分離原(yuan)理,而(er)是與(yu)被(bei)蒸餾混合物(wu)的分(fen)子量的大小(xiao)有關,能(neng)夠實現遠(yuan)離沸點下(xia)的操(cao)作(zuo),分子量差(cha)異越大,分子自由(you)程相(xiang)差(cha)越大,餾出物就越純(chun)。這裏的分(fen)子自由(you)程(用(yong)λ表示(shi))是指(zhi)壹(yi)個(ge)分(fen)子相鄰(lin)兩(liang)次碰撞(zhuang)之(zhi)間(jian)所走的路(lu)程。
在高真(zhen)空的條(tiao)件(jian)下(xia),液(ye)體(ti)混合物(wu)沿(yan)著(zhe)加熱(re)板(ban)流動(dong)被(bei)加熱(re),根(gen)據不(bu)同分子量物(wu)質的分(fen)子平均(jun)自由(you)程的不(bu)同,它們在汽化表(biao)面與(yu)冷凝表面之(zhi)間(jian)分(fen)子平均(jun)自由(you)程的大小(xiao)以及蒸發(fa)度(du)也明(ming)顯(xian)的不(bu)同,輕組(zu)分(fen)分(fen)子的分(fen)子平均(jun)自由(you)程的大,而(er)重組(zu)分(fen)分(fen)子的分(fen)子平均(jun)自由(you)程小(xiao),使(shi)得(de)輕組(zu)分(fen)恰(qia)好(hao)能(neng)到(dao)達(da)冷凝板(ban)上(shang)面被(bei)冷凝,使(shi)其沿(yan)冷凝板(ban)留(liu)下(xia);而(er)重組(zu)分(fen)分(fen)子因達不到(dao)冷凝板(ban)而(er)沿(yan)著(zhe)加熱(re)板(ban)留(liu)下(xia),從而(er)將不同物質進(jin)行分(fen)離。
Molecular distillation is a special liquid-liquid separation technology. It is different from traditional distillation. It depends on the boiling point difference separation principle, but is related to the molecular weight of the distilled mixture. It can realize the operation far away from the boiling point. The greater the molecular weight difference, the greater the molecular free path difference, and the purer the distillate. The molecular free path here λ Is the distance traveled between two adjacent collisions of a molecule.
Under the condition of high vacuum, the liquid mixture flows along the heating plate and is heated. According to the different molecular average free path of substances with different molecular weight, the size and degree of evaporation of their molecular average free path between the vaporization surface and the condensation surface are also significantly different. The molecular average free path of light component molecules is large, while the molecular average free path of recombinant component molecules is small, So that the light component can just reach the condensing plate and be condensed, leaving it along the condensing plate; The recombinant molecules are left along the heating plate because they can not reach the condensing plate, so as to separate different substances.
分子蒸餾儀技(ji)術特點(dian)Technical Features:
分(fen)子蒸餾技術作(zuo)為壹(yi)種(zhong)與(yu)國(guo)際(ji)同步的高(gao)新(xin)分離技術,具(ju)有其他分離技術沒(mei)有的優(you)點:
1.遠低(di)於物料(liao)沸點的溫(wen)度(du)下(xia)操(cao)作(zuo),而(er)且物料(liao)停(ting)留(liu)時間(jian)短(duan);利於(yu)高(gao)沸點、熱(re)敏(min)及(ji)易(yi)氧化物(wu)料(liao)的分(fen)離;
2.有效地(di)脫(tuo)除(chu)液(ye)體(ti)中(zhong)的物(wu)質如(ru)有機溶劑(ji)、臭(chou)味(wei)等,對於采(cai)用(yong)溶劑(ji)萃取後(hou)液(ye)體(ti)的脫(tuo)溶是非常有效的方(fang)法;
3.可有選擇蒸發(fa)產出物,去除(chu)其(qi)它雜(za)質,通過(guo)多(duo)級分離可同時分離2種以上(shang)的物(wu)質;
4. 可有效地(di)脫(tuo)除(chu)輕分(fen)子物質(脫(tuo)臭(chou))、重分子物質(脫(tuo)色(se))及(ji)脫(tuo)除(chu)混合物(wu)中(zhong)雜(za)質;
5.其分離過(guo)程為物(wu)理分(fen)離過(guo)程,可(ke)很好(hao)地保(bao)護被(bei)分(fen)離物質不被(bei)汙(wu)染(ran),特別(bie)是可保(bao)持(chi)天然提(ti)取物原(yuan)來的品(pin)質;
6.沒(mei)有沸騰(teng)鼓(gu)泡(pao)現象(xiang),分(fen)子蒸餾是液(ye)層(ceng)表面上(shang)的自由(you)蒸發(fa),在低(di)壓(ya)力下(xia)進(jin)行,液(ye)體(ti)中(zhong)無(wu)溶(rong)解(jie)的空氣,因(yin)此在蒸餾過(guo)程中(zhong)不(bu)能(neng)使(shi)整個(ge)液(ye)體(ti)沸騰(teng),沒(mei)有鼓(gu)泡(pao)現象(xiang);
7. 分(fen)離度(du)高,高(gao)於傳統蒸餾及普(pu)通的薄(bo)膜(mo)蒸發(fa)器(qi);
8.容易(yi)形(xing)成連(lian)續(xu)化(hua)生產,操(cao)作(zuo)簡(jian)單;
9.分(fen)子蒸餾的蒸程短(duan),分子平均(jun)自由(you)程壹(yi)般不超過(guo)25mm,能(neng)耗(hao)小(xiao)。
10.進(jin)料(liao)罐可選實現預(yu)加熱(re)功能(neng),預(yu)熱(re)溫(wen)度(du)可以調節;
11.各(ge)個接(jie)口采(cai)用(yong)的是氟膠墊(dian)片(pian)進(jin)行密(mi)封,氣密性好(hao),如(ru)客(ke)戶需要耐(nai)腐(fu)蝕(shi)可以更換成(cheng)四氟材質。
As a high-tech separation technology synchronized with the world, molecular distillation technology has incomparable advantages over other separation technologies:
1. Operate at a temperature far below the boiling point of the material, and the residence time of the material is short; It is conducive to the separation of high boiling point, heat sensitive and easily oxidized materials;
2. Effectively remove substances in liquid, such as organic solvent and odor, which is a very effective method for the desolvation of liquid after solvent extraction;
3. The product can be evaporated selectively to remove other impurities. More than 2 substances can be separated at the same time through multistage separation;
4. It can effectively remove light molecular substances (deodorization), heavy molecular substances (decolorization) and impurities in the mixture;
5. The separation process is a physical separation process, which can well protect the separated substances from pollution, especially maintain the original quality of the natural extract;
6. There is no boiling and bubbling phenomenon. Molecular distillation is free evaporation on the surface of the liquid layer. It is carried out under low pressure and there is no dissolved air in the liquid. Therefore, the whole liquid cannot boil and there is no bubbling phenomenon in the distillation process;
7. High separation, higher than traditional distillation and ordinary thin film evaporator;
8. Easy to form continuous production and simple operation;
9. Molecular distillation has a short evaporation range, the average free path of the molecule is generally no more than 25mm, and the energy consumption is small.
10. The feed tank can optionally realize the pre heating function, and the preheating temperature can be adjusted;
11. Each interface is sealed with fluororubber gasket with good air tightness. If the customer needs corrosion resistance, it can be replaced with Teflon material.
應用(yong)範圍(wei)Application Scope:
l 可(ke)代替常(chang)規(gui)降(jiang)膜蒸發(fa)器(qi),用(yong)於石(shi)化(hua)及(ji)化(hua)工產品(pin)的蒸餾、提純(chun)、濃(nong)縮(suo)、脫(tuo)色(se)使(shi)用(yong);
l 尤其(qi)適(shi)用(yong)於熱(re)敏(min)性(xing),易(yi)氧化化(hua)學(xue)工(gong)業品(pin)的蒸餾精(jing)制(zhi);
l 也(ye)可(ke)用(yong)於高(gao)沸點產品(pin)的蒸餾分離;
l instead of conventional falling film evaporator, it can be used for distillation, purification, concentration and decolorization of petrochemical and chemical products;
l it is especially suitable for distillation and refining of heat sensitive and easily oxidized chemical industrial products;
l it can also be used for distillation and separation of products with high boiling point;
典(dian)型應(ying)用(yong)Typical Applications:
l 多不(bu)飽和脂肪(fang)酸(油酸、亞(ya)麻酸(suan)、魚(yu)油脂(zhi)肪(fang)酸(乙(yi)酯)及其(qi)衍(yan)生物(wu)的蒸餾精(jing)制(zhi);
l 單甘脂的精(jing)制(zhi);
l 二(er)聚酸的精(jing)制(zhi);
l VE、植(zhi)物(wu)甾醇的精(jing)制(zhi);
l 液(ye)晶的蒸餾;
l 高分(fen)子聚合物(wu)脫(tuo)除(chu)單體(ti);
l 其(qi)他熱(re)敏(min)性(xing)產品(pin)的精(jing)制(zhi);
l distillation and refining of polyunsaturated fatty acids (oleic acid, linolenic acid, fish oil fatty acid (ethyl ester) and their derivatives;
l refining of monoglyceride;
l refining of dimer acid;
l refining of VE and phytosterol;
l distillation of liquid crystal;
l monomer removal by high polymer;
l refining of other heat sensitive products;
產品(pin)選型Product Selection
短(duan)程蒸餾的處(chu)理能(neng)力和原(yuan)料(liao)(產品(pin))的分(fen)子量,物(wu)料(liao)粘(zhan)度(du)、操(cao)作(zuo)條(tiao)件(jian)、蒸發(fa)器(qi)的有效換(huan)熱(re)面積有直接(jie)關系(xi)。
常(chang)用(yong)進(jin)料(liao)速(su)率(lv):50-80 kg / (m²*h)
可選(xuan)材質:SUS304,SUS316L,SAF2205
工作(zuo)溫度(du):最高(gao)近400℃
The processing capacity of short-range distillation is directly related to the molecular weight of raw materials (products), material viscosity, operating conditions and effective heat exchange area of evaporator.
Common Feed Rate: 50-80 kg / (m²*h)
Optional Materials: SUS304, SUS316L, SAF2205
Operating Temperature: up to nearly 400 ℃
產品(pin)型號/Product Model | MSPE80 | MSPE100 | MSPE150 | MSPE200 | MSPE230 | MSPE10M | MSPE20M | MSPE30M |
蒸發(fa)面積/Evaporation Area | 0.1㎡ | 0.15㎡ | 0.25㎡ | 0.35㎡ | 0.5㎡ | 0.8㎡ | 1㎡ | 2㎡ |
冷凝面積/Condensation Area | 0.15㎡ | 0.25㎡ | 0.45㎡ | 0.55㎡ | 0.65㎡ | 1.0㎡ | 1.5㎡ | 3㎡ |
進(jin)料(liao)容積 /Feed Volume | 10L | 10L | 15L | 20L | 50L | 100L | 100L | 200L |
電(dian)機功率(lv)/Motor Power | 120W | 120W | 120W | 180W | 370W | 750W | 1100W | 1500W |
最大轉(zhuan)速(su)/Maximum Speed | 50~450rpm | |||||||
輕組(zu)分(fen)收(shou)集(ji)瓶(ping)/Light Component Collection Bottle | 1L | 2L | 3L | 10L | 30L | 50L | 50L | 100L |
重組(zu)分(fen)收(shou)集(ji)瓶(ping)/Recombinant Collection Bottle | 1L | 2L | 3L | 10L | 30L | 50L | 50L | 100L |
冷井/Cold Well | 有(have) | |||||||
冷卻裝置/Cooling System | 有(have) | |||||||
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